Analytical Electrochemistry: A Laboratory Manual
This labware module contains directions for seven experiments in analytical electrochemistry. The experiments are designed to illustrate fundamentals of electrode reactions as applied to readily accessible redox reactants. They provide insight to dynamic electrochemistry for scientists at all levels of training. Activation procedures to prepare glassy carbon electrodes are provided in a TechNote.
Synthesis of a Sonogel-Carbon Modified Sensor Electrode with Titanium Oxide (TiO2) to Detect Catecho
This experiment demonstrates cyclic voltammetry, surface modification, selectivity, and bioanalysis in assaying catechols in the presence of ascorbic acid. Pre- or post-lab questions are included, along with sample student data and instructor\'s notes.
Teaching Chemical Equilibrium Concepts Using Field-Lab Experiences
This online article describes an inquiry-based experience designed to integrate concepts in water quality and geology for pre-education science students preparing to become teachers at the primary and secondary level. The field and laboratory exercise could be used to effectively introduce equilibrium chemistry in an introductory or environmental chemistry course, and courses for non-majors.
Electrochemistry and Detection of Organic and Biological Molecules such as Catechols
This ASDL online article describes a lab experiment whereby students learn how to prepare a conducting thin-film polymer electrode for the analysis of catechol and the effect of ascorbic acid on the cyclic voltammetric results.
Kinetic Capillary Electrophoresis(KCE): A conceptual Platform for Kinetic Homogeneous Affinity Metho
Kinetic Capillary Electrophoresis is a family of methods for studying binding of biopolymers, measuring rate constants, binding constants, and in some cases providing mechanistic details. This Online Article is a presentation by the originators of this family of techniques ready for classroom or independent use.
Active Learning in Advanced Analytical Chemistry, a course for first year graduate students
The introductory lecture course for graduate-level analytical chemistry is commonly understood to require students to be broadly aware of analytical tools, current problems, and methods for linking problems and measurements. This article describes an active learning approach to this course, using review articles to focus discussion and reveal gaps in student knowledge. Students give most of the course\'s lectures, with grades based on lectures, exams, and a term paper.
Animation of Dual Head HPLC Pump
This animation site deals specifically with dual head LC pumping. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL.
Animation of sample loop HPLC injections
This site deals specifically with sample loop injections in liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are listed below.
Animation of GC solvent focusing
This site has very good animations related to separations. It deals specifically with solvent focusing in gas chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL.
Animation of diode array detection in HPLC
This animation site deals specifically with diode array detection for liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. This site requires FLASH version 7 or
Animation of GC flame ionization detector
This site is one in a series of sites with very good animations related to separations. This animation deals specifically with flame ionization detection in GC. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (T
GC coating animation
This site is one in a series of sites with very good animations related to separations. This animation deals specifically with solute retention in GC. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are a
GC Splitless Injection Animation
This site is one in a series of sites with very good animations related to separations. This animation deals specifically with splitless injection in GC. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) ar
Chromatography books
This site simply offers books covering a wide range of both general and specific topics related to gas chromatography and its applications. While not of immediate pedagogical value, it may be useful to those looking for good texts about gas chromatography either for their own research needs or to provide as resources to their students.
Affinity Chromatography
Using exposition, graphics, and commercial videos, this module teaches the theory and application of affinity chromatography in the characterization of proteins, nucleic acids, and other biochemical/biomedical systems. Problems and application examples support the tutorial material.
PMT HandBook
This commercial site is an extensive description of the fundamentals and applications of photomultipliers including their characteristics, structures, operating parameters, and applications areas. The contents are provided in 14 chapters covering 323 pages that include nearly everything that you ever wanted to know about photomultiplier tubes. Reading the text and accompanying illustrations with patience and care, you can become an expert on the subject. It will allow the practitioner to use th
Analytical Electrochemistry: Basic concepts
This module focuses on the basic concepts involved in dynamic electrochemistry when the net current is not zero - the combination of mass transfer and electrochemical reactions at the interface between solids and fluids. It is at an introductory level appropriate for undergraduates in their sophomore or junior years.
Adopting POGIL Methodology for Analytical Chemistry
POGIL (Process Oriented Guided Inquiry Learning) is a NSF sponsored project designed to actively engage students in the learning process in the classroom. Ana-POGIL activities cover topics ranging from statistics to equilibria and to instrumentation. Materials are intended to have students work in groups on activities; each activity is structured in such a way that each concept is divided into a series of leading questions that allow the team to work through the concept. Answer keys can be re
RSC.org: UV/Vis Spectroscopy
This video distributed on YouTube is on the basic principles of UV/Vis. Provides a good primer (~5 min), and the “top-off” look of the instrument is useful in explaining components. A double beam instrument is described.
RSC.org: IR Spectroscopy
This video on YouTube covers the basic principles of infrared spectroscopy. Very useful for a newcomer to IR. This video of 6.5 minute would be useful in a classroom setting or students interested in the technique.
